NOP - Sustainability in the organic chemistry lab course

Cyclohexene

H₂O₂ / HCO₂H

reacts to

trans-1,2-Cyclohexanediol

; Side reactions

¹H-NMR

1H NMR

¹H-NMR: crude product
500 MHz, CDCl₃
delta [ppm]	mult.	atoms	assignment
1.21	m	4 H	4-H, 5-H
1.65	m	2 H	3-H, 6-H (axial)
1.92	m	2 H	3-H, 6-H (equatorial)
3.30	m	2 H	1-H, 2-H
4.15	s	1 H	OH
7.26	s	1 H	CHCl₃

1H NMR

¹H-NMR: trans-1,2-Cyclohexanediol
500 MHz, CDCl₃
delta [ppm]	mult.	atoms	assignment
1.21	m	4 H	4-H, 5-H
1.65	m	2 H	3-H, 6-H (axial)
1.92	m	2 H	3-H, 6-H (equatorial)
3.30	m	2 H	1-H, 2-H
4.15	s	1 H	OH
7.26	s	1 H	CHCl₃