| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
| + |
|
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|
; Side reactions |
13C-NMR |
| 13C-NMR: crude product | |||
| 75.5 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 13.79 | CH3 ethyl | ||
| 19.29 | C4 (ring) | ||
| 26.74 | C5 (ring) | ||
| 29.59 | C4 (3-oxobutyl) | ||
| 33.97 | C1 (3-oxobutyl) | ||
| 37.66 | C2 (3-oxobutyl) | ||
| 38.58 | C3 (ring) | ||
| 58.70 | C1 (ring) | ||
| 61.10 | CH2 ethyl | ||
| 171.07 | -C(=O)O- | ||
| 207.37 | C3 (C=O, 3-oxobutyl) | ||
| 214.46 | C2 (C=O, ring) | ||
| 76.5-77.5 | CDCl3 | ||
| 13C-NMR: 2-(3-Oxobutyl)cyclopentanone-2-carboxylic acid ethyl ester | |||
| 75.5 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 13.79 | CH3 ethyl | ||
| 19.29 | C4 (ring) | ||
| 26.74 | C5 (ring) | ||
| 29.59 | C4 (3-oxobutyl) | ||
| 33.97 | C1 (3-oxobutyl) | ||
| 37.66 | C2 (3-oxobutyl) | ||
| 38.58 | C3 (ring) | ||
| 58.70 | C1 (ring) | ||
| 61.10 | CH2 ethyl | ||
| 171.07 | -C(=O)O- | ||
| 207.37 | C3 (C=O, 3-oxobutyl) | ||
| 214.46 | C2 (C=O, ring) | ||
| 76.5-77.5 | CDCl3 | ||