| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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; Side reactions |
13C-NMR |
| 13C-NMR: crude product | |||
| 75.5 MHz, CDCl3, TMS | |||
| delta [ppm] | assignment | ||
| 25.98 | CH3 acetyl | ||
| 55.15 | -O-CH3 | ||
| 113.43 | C3 | ||
| 130.09 | C1 | ||
| 130.29 | C2 | ||
| 163.25 | C4 | ||
| 196.34 | C=O | ||
| 76.5-77.5 | CDCl3 | ||
| 120.8 | C4 (educt anisole) | ||
| 129.5 | C3 (educt anisole) | ||
| 13C-NMR: p-Methoxyacetophenone | |||
| 75.5 MHz, CDCl3, TMS | |||
| interactive spectrum | |||
| delta [ppm] | assignment | ||
| 25.98 | CH3 acetyl | ||
| 55.15 | -O-CH3 | ||
| 113.43 | C5 | ||
| 130.09 | C1 | ||
| 130.29 | C2 | ||
| 163.25 | C4 | ||
| 196.34 | C=O | ||
| 76.5-77.5 | CDCl3 | ||
| 120.8 | C4 (educt anisole) | ||
| 129.5 | C3 (educt anisole) | ||