NOP-Nr:
Alternative:
1035
Overview
Instructions
Operating scheme
Substances
Equipment
Evaluation
Analytics
- Chromatogram
-
1
H-NMR
-
13
C-NMR
- IR
+
Zeolith H-BEA 25
+
; Side reactions
Chromatogram
GC: crude product
column
DB-1, L=28 m, d=0.32 mm, film=0.25 µm
inlet
on column injection, 0.2 µL
carrier gas
H2, 40 cm/s
oven
40°C (5 min), 10°C/min --> 240°C (30 min)
detector
FID, 270°C
integration
percent concentration calculated from relative peak area
GC: pure product
column
DB-1, L=28 m, d=0.32 mm, film=0.25 µm
inlet
on column injection, 0.2 µL
carrier gas
H2, 40 cm/s
oven
40°C (5 min), 10°C/min --> 240°C (30 min)
detector
FID, 270°C
integration
percent concentration calculated from relative peak area
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pages/experiment.php: November 09, 2022
views/chromatogram.php: November 09, 2022