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NOP-Nr:
Overview
Instructions
Operating scheme
Substances
Equipment
Evaluation
Analytics
- 1H-NMR
- 13C-NMR
- IR
Cinchonidine + Benzyl chloride
acetone
reacts to
 (-)-N-Benzylcinchonidinium chloride ; Side reactions

13C-NMR

13C NMR
13C-NMR: crude product
75.5 MHz, MeOD
delta [ppm]assignment
22.5
25.9
28.0
39.1
52.7
62.0
65.2CH2 benzyl
66.2
69.7
117.5
121.4
124.2
126.1
128.8
129.1
130.3
131.1
131.7
134.9
138.7
147.6
148.7
151.0
47-50CH3OD

13C NMR
13C-NMR: (-)-N-Benzylcinchonidinium chloride
75.5 MHz, MeOD
delta [ppm]assignment
22.5
25.9
28.0
39.1
52.7
62.0
65.2CH2 benzyl
66.2
69.7
117.5
121.4
124.2
126.1
128.8
129.1
130.3
131.1
131.7
134.9
138.7
147.6
148.7
151.0
47-50CH3OD
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