| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - 1H-NMR |
| - 13C-NMR |
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| + |
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; Side reactions |
13C-NMR |
| 13C-NMR: crude product | |||
| 75.5 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 110.9 | C1 | ||
| 117.7 | C3 | ||
| 124.0 | C6 | ||
| 124.2 | C8 | ||
| 127.4 | C7 | ||
| 128.3 | C5 | ||
| 129.4 | C4 | ||
| 131.3 | C4a | ||
| 133.4 | C8a | ||
| 152.7 | C2 (C-OH) | ||
| 76.5-77.5 | CDCl3 | ||
| 13C-NMR: (R)-2,2'-Dihydroxy-1,1'-binaphthyl | |||
| 75.5 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 110.9 | C1 | ||
| 117.7 | C3 | ||
| 124.0 | C6 | ||
| 124.2 | C8 | ||
| 127.4 | C7 | ||
| 128.3 | C5 | ||
| 129.4 | C4 | ||
| 131.3 | C4a | ||
| 133.4 | C8a | ||
| 152.7 | C2 (C-OH) | ||
| 76.5-77.5 | CDCl3 | ||
| 13C-NMR: (S)-2,2'-Dihydroxy-1,1'-binaphthyl | |||
| 75.5 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 110.9 | C1 | ||
| 117.7 | C3 | ||
| 124.0 | C6 | ||
| 124.2 | C8 | ||
| 127.4 | C7 | ||
| 128.3 | C5 | ||
| 129.4 | C4 | ||
| 131.3 | C4a | ||
| 133.4 | C8a | ||
| 152.7 | C2 (C-OH) | ||
| 76.5-77.5 | CDCl3 | ||