NOP-Nr:
Overview
Instructions
Operating scheme
Substances
Equipment
Evaluation
Analytics
- Chromatogram
-
1
H-NMR
-
13
C-NMR
- IR
+
+ NaOH
+ Adogen 464
+
; Side reactions
13
C-NMR
13
C-NMR: crude product
75.5 MHz, CDCl
3
delta [ppm]
assignment
14.0
C12
22.7
C11
67.9
C1
114.5
C2, C6 (ring)
1204
C4 (ring)
129.4
C3, C5 (ring)
159.2
C1 (ring)
76.5-77.5
CDCl
3
13
C-NMR: Dodecyl phenyl ether
75.5 MHz, CDCl
3
delta [ppm]
assignment
14.0
C12
22.7
C11
67.9
C1
114.5
C2, C6 (ring)
1204
C4 (ring)
129.4
C3, C5 (ring)
159.2
C1 (ring)
76.5-77.5
CDCl
3
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pages/experiment.php: November 09, 2022
views/cnmr.php: November 09, 2022