NOP - Sustainability in the organic chemistry lab course

1-Bromododecane

+

Phenol

+ NaOH
+ Adogen 464

reacts to

Dodecyl phenyl ether

+

Sodium bromide

; Side reactions

¹H-NMR

1H NMR

¹H-NMR: crude product
300 MHz, CDCl₃
delta [ppm]	mult.	atoms	assignment
0.88	t	3 H	12-H
1.27	m	16 H	4-CH₂ - 11-CH₂
1.44	m	2 H	3-H
1.75	m	2 H	2-H
3.91	t	2 H	1-H
6.88	m	3 H	2-H, 4-H, 6-H (phenyl)
7.25	dd	2 H	3-H, 5-H (phenyl)

1H NMR

¹H-NMR: Dodecyl phenyl ether
300 MHz, CDCl₃
delta [ppm]	mult.	atoms	assignment
0.88	t	3 H	12-H
1.27	m	16 H	4-CH₂ - 11-CH₂
1.44	m	2 H	3-H
1.75	m	2 H	2-H
3.91	t	2 H	1-H
6.88	m	3 H	2-H, 4-H, 6-H (phenyl)
7.25	dd	2 H	3-H, 5-H (phenyl)