NOP-Nr:
Overview
Instructions
Operating scheme
Substances
Equipment
Evaluation
Analytics
- Chromatogram
-
1
H-NMR
-
13
C-NMR
- IR
+
NaOH
+
+
; Side reactions
Chromatogram
GC: crude product
column
Zebron ZB-1, L=15 m, d=0.25 mm, película=0.25 µm
inlet
injector: 280°C, inyección partida, 0.1 µL
carrier gas
H2, presión previa de la columna 150 kPa
oven
30 °C (2 min), 8°C/min --> 250°C (2 min)
detector
FID, 300°C, H2 25.1 mL/min, synth. air 393 mL/min
integration
percent concentration calculated from relative peak area
GC: pure product
column
Zebron ZB-1, L=15 m, d=0.25 mm, película=0.25 µm
inlet
injector: 280°C, inyección partida, 0.1 µL
carrier gas
H2, presión previa de la columna 150 kPa
oven
30 °C (2 min), 8°C/min --> 250°C (2 min)
detector
FID, 300°C, H2 25.1 mL/min, synth. air 393 mL/min
integration
percent concentration calculated from relative peak area
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pages/experiment.php: 09 Nov 2022
views/chromatogram.php: 09 Nov 2022