| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
| + |
|
|
| + |
| + |
|
; Side reactions |
13C-NMR |
| 13C-NMR: Cinnamic acid methyl ester | |||
| 300 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 51.36 | O-CH3 (cis-) | ||
| 51.69 | O-CH3 (trans-) | ||
| 117.80 | C2 (trans-) | ||
| 119.28 | C2 (cis-) | ||
| 128.03 | C-H aromático | ||
| 128.07 | C-H aromático | ||
| 128.88 | C-H aromático | ||
| 129.08 | C-H aromático | ||
| 129.71 | C-H aromático | ||
| 130.29 | C-H aromático | ||
| 134.39 | C1 (aromático, trans-) | ||
| 134.76 | C1 (aromático, cis-) | ||
| 143.39 | C3 (cis-) | ||
| 144.86 | C3 (trans-) | ||
| 166.48 | C1 (-C(=O)O-, cis-) | ||
| 167.41 | C1 (-C(=O)O-, trans-) | ||
| 76.5-77.5 | CDCl3 | ||