| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
|
|
|
; Side reactions |
Chromatogram |
| GC: pure product | |
| column | DB-1, L=28 m, d=0.32 mm, película=0.25 µm |
| inlet | inyección en la columna |
| carrier gas | H2, 40 cm/s |
| oven | 90°C (5 min), 10°C/min --> 240°C (30 min) |
| detector | FID, 270°C |
| integration | percent concentration calculated from relative peak area |