| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
|
|
|
; Side reactions |
13C-NMR |
| 13C-NMR: crude product | |||
| 75.5 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 111.0 | C1 | ||
| 117.8 | C3 | ||
| 124.0 | C6 | ||
| 124.2 | C8 | ||
| 127.5 | C7 | ||
| 128.4 | C5 | ||
| 129.6 | C4 | ||
| 131.4 | C4a | ||
| 133.5 | C8a | ||
| 152.8 | C2 | ||
| 76.5-77.5 | CDCl3 | ||
| 13C-NMR: 2,2'-Dihidroxi-1,1'-binaftilo | |||
| 75.5 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 111.0 | C1 | ||
| 117.8 | C3 | ||
| 124.0 | C6 | ||
| 124.2 | C8 | ||
| 127.5 | C7 | ||
| 128.4 | C5 | ||
| 129.6 | C4 | ||
| 131.4 | C4a | ||
| 133.5 | C8a | ||
| 152.8 | C2 | ||
| 76.5-77.5 | CDCl3 | ||