| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
|
|
|
; Side reactions |
13C-NMR |
| 13C-NMR: crude product | |||
| 125 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 14.0 | C8 | ||
| 22.6 | C7 | ||
| 25.7 | C6 | ||
| 29.2 | C5 | ||
| 29.4 | C4 | ||
| 31.8 | C3 | ||
| 32.6 | C2 | ||
| 63.0 | C1 | ||
| 76.5-77.5 | CDCl3 | ||
| 13C-NMR: 1-Octanol | |||
| 125 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 14.0 | C8 | ||
| 22.6 | C7 | ||
| 25.7 | C6 | ||
| 29.2 | C5 | ||
| 29.4 | C4 | ||
| 31.8 | C3 | ||
| 32.6 | C2 | ||
| 63.0 | C1 | ||
| 76.5-77.5 | CDCl3 | ||