NOP-Nr:
Overview
Instructions
Operating scheme
Substances
Equipment
Evaluation
Analytics
- Chromatogram
-
1
H-NMR
-
13
C-NMR
- IR
1. NaBH
4
, I
2
H
2
O
2
/ NaOH
; Side reactions
1
H-NMR
1
H-NMR: crude product
500 MHz, CDCl
3
delta [ppm]
mult.
atoms
assignment
0.85
t (
3
J = 6.7 Hz)
3 H
CH
3
1.19-1.34
m
10 H
CH
2
C3-C7
1.49-1.57
m
2 H
CH
2
C2
2.34
broad s
1 H
O-H
3.60
t (
3
J = 6.7 Hz)
2 H
CH
2
-O-
7.26
s
1 H
CHCl
3
1
H-NMR: 1-Octanol
500 MHz, CDCl
3
delta [ppm]
mult.
atoms
assignment
0.85
t (
3
J = 6.7 Hz)
3 H
CH
3
1.19-1.34
m
10 H
CH
2
C3-C7
1.49-1.57
m
2 H
CH
2
C2
2.34
broad s
1 H
O-H
3.60
t (
3
J = 6.7 Hz)
2 H
CH
2
-O-
7.26
s
1 H
CHCl
3
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pages/experiment.php: 09 Nov 2022
views/hnmr.php: 09 Nov 2022