| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
|
|
|
; Side reactions |
Chromatogram |
| TLC: crude product | |
| TLC layer | Merck silica gel 60 F254 |
| mobile phase | EtOAc |
| detection | immerse into solution of 2.7 g KMnO4, 18 g K2CO3, 216 mg NaOH in 274 mL H2O, heating with air dryer |
| Rf (educt) | 0.87 |
| Rf (product) | 0.67 |