| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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; Side reactions |
1H-NMR |
| 1H-NMR: crude product | |||
| 250 MHz, DMSO-d6 | |||
| delta [ppm] | mult. | atoms | assignment |
| 0.86 | t (3J = 6.4 Hz) | 3 H | CH3 |
| 1.2-1.6 | m | 26 H | other CH2 |
| 2.18 | t (3J = 7.3 Hz) | 2 H | 2-CH2 |
| 3.25 | m | 2 H | 9-CH-OH, 10-CH-OH |
| 2.45 | s | 6 H | DMSO |
| 1H-NMR: erythro-9,10-Dihydroxystearic acid | |||
| 250 MHz, DMSO-d6 | |||
| delta [ppm] | mult. | atoms | assignment |
| 0.86 | t (3J = 6.4 Hz) | 3 H | CH3 |
| 1.2-1.6 | m | 26 H | other CH2 |
| 2.18 | t (3J = 7.3 Hz) | 2 H | 2-CH2 |
| 3.25 | m | 2 H | 9-CH-OH, 10-CH-OH |
| 2.45 | s | 6 H | DMSO |