| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
|
|
|
; Side reactions |
13C-NMR |
| 13C-NMR: crude product | |||
| 62.5 MHz, DMSO-d6, 373°K | |||
| delta [ppm] | assignment | ||
| 13.0 | C18 (CH3) | ||
| 21.2 | C17 (CH2 | ||
| 23.9 | CH2 | ||
| 24.8 | CH2 | ||
| 27.9 | CH2 | ||
| 28.0 | CH2 | ||
| 28.3 | CH2 | ||
| 28.4 | CH2 | ||
| 28.6 | CH2 | ||
| 30.6 | CH2 | ||
| 31.8 | CH2 | ||
| 33.2 | C2 | ||
| 73.4 | C9, C10 (CH-OH) | ||
| 173.4 | C1 (COOH) | ||
| 38.5-40.5 | DMSO-d6 | ||
| 13C-NMR: erythro-9,10-Dihydroxystearic acid | |||
| 62.5 MHz, DMSO-d6, 373°K | |||
| delta [ppm] | assignment | ||
| 13.0 | C18 (CH3) | ||
| 21.2 | C17 (CH2 | ||
| 23.9 | CH2 | ||
| 24.8 | CH2 | ||
| 27.9 | CH2 | ||
| 28.0 | CH2 | ||
| 28.3 | CH2 | ||
| 28.4 | CH2 | ||
| 28.6 | CH2 | ||
| 30.6 | CH2 | ||
| 31.8 | CH2 | ||
| 33.2 | C2 | ||
| 73.4 | C9, C10 (CH-OH) | ||
| 173.4 | C1 (COOH) | ||
| 38.5-40.5 | DMSO-d6 | ||