NOP-Nr:
Alternative:
4010
Overview
Instructions
Operating scheme
Substances
Equipment
Evaluation
Analytics
- Chromatogram
-
1
H-NMR
-
13
C-NMR
- IR
+
Sc(OTf)
3
+
; Side reactions
Chromatogram
GC: crude product
column
5CB Low Blend/MS, L=20 m, d=0.32 mm, film=0.25 µm
inlet
injector: 210°C, split injection, 1 µL
carrier gas
H2, pre-column pressure 50 kPa
oven
60°C (2 min), 10°C/min --> 240°C (30 min)
detector
FID, 310°C
integration
percent concentration calculated from relative peak area
GC: pure product
column
5CB Low Blend/MS, L=20 m, d=0.32 mm, film=0.25 µm
inlet
injector: 210°C, split injection 1 µL
carrier gas
H2, pre-column pressure 50 kPa
oven
60°C (2 min), 10°C/min --> 240°C (30 min)
detector
FID, 310°C
integration
percent concentration calculated from relative peak area
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pages/experiment.php: November 09, 2022
views/chromatogram.php: November 09, 2022