| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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; Side reactions |
Chromatogram |
| GC: crude product | |
| column | HP-5, L=30 m, d=0.32 mm, film=0.25 µm |
| inlet | split injection 1:194, 3 µL |
| carrier gas | H2, pre-column pressure 31 kPa |
| oven | 50°C (3 min), 8°C/min --> 320°C |
| detector | FID, 300°C |
| integration | percent concentration calculated from relative peak area |
| GC: pure product | |
| column | HP-5, L=30 m, d=0.32 mm, film=0.25 µm |
| inlet | split injection 1:194, 3 µL |
| carrier gas | H2, pre-column pressure 31 kPa |
| oven | 50°C (3 min), 8°C/min --> 320°C |
| detector | FID, 300°C |
| integration | percent concentration calculated from relative peak area |