| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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; Side reactions |
Chromatogram |
| GC: crude product | |
| column | Zebron ZB-1, L=15 m, d=0.25 mm, film 0.25 µm (Phenomenex) |
| inlet | injector: 250°C, split injection, 0.15 µL |
| carrier gas | He, pre-column pressure 101 kPa |
| oven | 85°C (0 min), 8°C/min --> 250°C (10 min) |
| detector | FID, 250°C, H2 33.9 mL/min, synth. air 322 mL/min, isocratic N2, 15 mL/min (59 kPa) |
| integration | percent concentration calculated from relative peak area |
| GC: pure product | |
| column | Zebron ZB-1, L=15 m, d=0.25 mm, film 0.25 µm (Phenomenex) |
| inlet | injector: 250°C, split injection, 0.15 µL |
| carrier gas | He, pre-column pressure 101 kPa |
| oven | 85°C (0 min), 8°C/min --> 250° C (10 min) |
| detector | FID 250°C, H2 33.9 mL/min, synth. air 322 mL/min, isocratic N2, flow 15 mL/min (59 kPa) |
| integration | percent concentration calculated from relative peak area |